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Response surface optimization and support vector regression modeling of microwave-assisted essential oil extraction from cumin seeds
(Elsevier BV, 2024-02)
Ali Asif Khan
;
Sadaf Zaidi
;
Fazil Qureshi
;
Mohammad Yusuf
;
Abdullah A. Al-Kahtani
The current research involved creating models using Response Surface Methodology (RSM) and Support Vector Regression (SVR) to forecast the amount of extractable essential oil that can be obtained from powdered cumin seeds. Influence of microwave power (140–280–420–560–700 W), amount of water (500–600–700–800–900 ml), duration of distillation (30–45–60–75–90 min) and soak time (15–30–45–60–75 min) on essential oil yield were investigated. Microwave Assisted Extraction (MAE) allowed higher recoveries compared to conventional Soxhlet extraction, without altering the chemical components of the extract. A five-level four FCC experimental design was developed using Minitab (15.1.20.0). A total of 31 runs were performed in microwave-assisted extraction apparatus. Experimental data obtained was then used for developing RSM and SVR models for the prediction of the yield of essential oil. The optimum conditions for maximum yield of cumin oil were given by RSM. Maximum yield of 3.4 ml (0.017 ml/g) was found at 140 W of microwave power, 500 ml of water, 90 min duration of distillation, and 15 min of soak time. In this work, epsilon SVR with RBF kernel was used. The grid search (depth-first search) methodology was applied for tuning the values of epsilon, gamma, and cost using the LIBSVM module on the MATLAB interface. The statistical parameters namely, average absolute relative error (AARE), coefficient of determination (R2), standard deviation (SD), and root mean square error (RMSE) were selected as the performance parameters. The developed SVR model was compared with the RSM model. The AARE values of 2.27% and 1.29%, R2 values of 0.86 and 0.99, SD values of 1.73 and 0.29, and RMSE values of 0.0284 and 0.0132 were obtained for RSM and SVR models respectively. It is found that SVR is more accurate and better tool for modeling of MAE process.
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Optimization of syngas production from co-gasification of palm oil decanter cake and alum sludge: An RSM approach with char characterization
(Elsevier BV, 2024-04)
Kunmi Joshua Abioye
;
Noorfidza Yub Harun
;
Suriati Sufian
;
Mohammad Yusuf
;
Ahmad Hussaini Jagaba
The study explores co-gasification of palm oil decanter cake and alum sludge, investigating the correlation between input variables and syngas production. Operating variables, including temperature (700–900 °C), air flow rate (10–30 mL/min), and particle size (0.25–2 mm), were optimized to maximize syngas production using air as the gasification agent in a fixed bed horizontal tube furnace reactor. Response Surface Methodology with the Box-Behnken design was used employed for optimization. Fourier Transformed Infra-Red (FTIR) and Field Emission Scanning Electron Microscopic (FESEM) analyses were used to analyze the char residue. The results showed that temperature and particle size have positive effects, while air flow rate has a negative effect on the syngas yield. The optimal CO + H2 composition of 39.48 vol% was achieved at 900 °C, 10 mL/min air flow rate, and 2 mm particle size. FTIR analysis confirmed the absence of C─Cl bonds and the emergence of Si─O bonds in the optimized char residue, distinguishing it from the raw sample. FESEM analysis revealed a rich porous structure in the optimized char residue, with the presence of calcium carbonate (CaCO3) and aluminosilicates. These findings provide valuable insights for sustainable energy production from biomass wastes.

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